Extended knowledge of 288-32-4

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 288-32-4.

288-32-4, Adding some certain compound to certain chemical reactions, such as: 288-32-4, name is 1H-Imidazole, can increase the reaction rate and produce products with better performance than tho

General procedure: To a vigorously stirred suspension of the CuNPs/MagSilica catalyst (100 mg) in DMF (6 mL) under air, K2CO3 (276 mg, 2.0 mmol) and imidazole (136 mg, 2.0 mmol) were added. The reaction mixture was stirred for 30 min and then the correspo

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 288-32-4.

Reference:
Article; Nador, Fabiana; Volpe, Maria Alicia; Alonso, Francisco; Radivoy, Gabriel; Tetrahedron; vol. 70; 36; (2014); p. 6082 – 6087;,
Jessica.FPosted on Categories 288-32-4, imidazoles-derivativesTags

New learning discoveries about 84946-20-3

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 84946-20-3.

84946-20-3, Adding some certain compound to certain chemical reactions, such as: 84946-20-3, name is 2-Chloro-1-(4-fluorobenzyl)-1H-benzo[d]imidazole, can increase the reaction rate and produce

Step C; 1-(4-fluorobenzyl) 2-piperazinyl benzimidazole In 168 ml xylene 40.8 g anhydrous piperazine and 60 g 2-chloro (4-fluorobenzyl) benzimidazole are added. The mixture is heated to 80 C. for 10 hours. When the reaction is no longer evoluting, the temp

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 84946-20-3.

Reference:
Patent; Laboratoire Theramex S.A.; US5461059; (1995); A;,
Imidazole – Wikipedia,
Jessica.FPosted on Categories 84946-20-3, imidazoles-derivativesTags

The origin of a common compound about 71759-89-2

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 71759-89-2.

These common heterocyclic compound, 71759-89-2, name is 5-Iodo-1H-imidazole, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below

General procedure: Method A: In a20 mL microwave Biotage tube, a mixture of 4-iodo-1H-imidazole(1a) (0.194 g, 1.0 mmol), a boronic acid 2(2.0 mmol), CsF (0.456 g,3.0 mmol), PdCl2(dppf)(0.041 g, 0.05 mmol) and BnEt3NCl(0.011 g, 0.05 mmol) in toluene(7 mL)

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 71759-89-2.

Reference:
Article; Vichier-Guerre, Sophie; Dugue, Laurence; Pochet, Sylvie; Tetrahedron Letters; vol. 55; 46; (2014); p. 6347 – 6350;,
Imidazole – Wikipedia,
Jessica.FPosted on Categories 71759-89-2, imidazoles-derivativesTags

Introduction of a new synthetic route about 5-Iodo-1-methyl-1H-imidazole

If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it.

71759-88-1, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale

[2075] EtMgBr (3Molar in Et2O) solution (791 uL), was dripped into a solution of 914 (0.518 g, 3.15 mmol, 6 eq.) in ClCH2CH2Cl (6 ML), for 30 minutes. To the white suspended mixture, 913b (0.280 g, 0.525 mmol) was then added and stirred at 60 C. for 3 hou

If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it.

Reference:
Patent; Zhu, Hugh Y.; Njoroge, F. George; Cooper, Alan B.; Guzi, Timothy; Rane, Dinanath F.; Minor, Keith P.; Doll, Ronald J.; Girijavallabhan, Viyyoor M.; Santhanam, B

Simple exploration of 288-32-4

The synthetic route of 288-32-4 has been constantly updated, and we look forward to future research findings.

288-32-4, A common heterocyclic compound, 288-32-4, name is 1H-Imidazole, molecular formula is C3H4N2, its traditional synthetic route has been very mature, but the traditional synthetic route ha

A mixture of imidazole (1 .36 g, 20.0 mmol) and sodium hydroxide (0.80 g, 20.0 mmol) in DMSO was heated to 90 C for 2 h, and then cooled to room temperature. A solution of 1 -bromooctane (3.46 g, 19.0 mmol) in DMSO was added dropwise to the mixture. After

The synthetic route of 288-32-4 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH; ZHANG, Yugen; YUAN, Yuan; (57 pag.)WO2018/56902; (2018); A1;,
Imidazole – Wikip

Research on new synthetic routes about 1H-Imidazole

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1H-Imidazole, other downstream synthetic routes, hurry up and to see.

Adding a certain compound to certain chemical reactions, such as: 288-32-4, name is 1H-Imidazole, belongs to imidazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional

Add 400 g of dichloromethane to a 1000 mL two-necked flask, and then pour into it200g imidazole, stir to fully dissolve,And place the reaction flask at 0 CIn the low temperature reactor, at this time, gradually add to the reaction flask86.2g of sulfonyl

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1H-Imidazole, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Zhuhai Saiwei Electronic Materials Co., Ltd.; Mao Chong; Xu Jiliang; Dai Xiaobing; (7 pag.)CN110305066; (2019); A;,
Jessica.FPosted on Categories 288-32-4, imidazoles-derivativesTags

Introduction of a new synthetic route about 1H-Imidazole

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 1H-Imidazole, and friends who are interested can also refer to it.

288-32-4, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual situ

General procedure: A mixture of p-nitro chlorobenzene 3 (25.0 g, 0.200 mol), appropriatesecondary amine 2a,b,e,f (0.300 mol) and anhydrous potassiumcarbonate (40.0 g) were mixed in DMF (300 mL), and thencatalytic drops of Aliquat 336 reagent were added. T

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 1H-Imidazole, and friends who are interested can also refer to it.

Reference:
Article; Abdel-Atty, Mona M.; Farag, Nahla A.; Kassab, Shaymaa E.; Serya, Rabah A.T.; Abouzid, Khaled A.M.; Bioorganic Chemistry; vol. 57; (2014); p. 65 – 82;,
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The important role of 2-Mercaptobenzimidazole

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583-39-1, Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions

Benzimid-azole-2-thione 1 (1.50 g, 10 mmol) and morpholine (0.87 ml, 0.87 g, 10 mmol) were dissolved in 2-PrOH (30 ml); 37% aqueous formaldehyde (0.90 ml, 12 mmol) was added, and the mixture was refluxed for 3 h (precipitate formed almost immediately). Th

If you are interested in these compounds, you can also browse my other articles.Thank you for taking the time to read this article. I hope you enjoyed it.

Reference:
Article; Bespalov; Gorchakova; Ivanov; Kuznetsov; Kuznetsova; Pankova; Prokopenko; Avdontceva; Chemistry of Heterocyclic Compounds; vol. 50; 11; (2015); p. 1547 – 1558;,
Jessica.FPosted on Categories 583-39-1, imidazoles-derivativesTags

Discovery of 4-Iodo-1-trityl-1H-imidazole

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 4-Iodo-1-trityl-1H-imidazole, and friends who are interested can also refer to it.

96797-15-8, As we all know, there are many different methods for the synthesis of a compound, and people can choose the synthesis method that suits their own laboratory according to the actual

A 2 M isopropylmagnesium chloride solution in THF (8.60 mL, 17.2 mmol) was added dropwise to a solution of 4-iodo-1-trityl-imidazole (5.00 g, 11.5 mmol) in anhydrous THF (55 mL) at 0 C under nitrogen. The resulting mixture was stirred at 0 C for 10 minute

At the same time, in my other blogs, there are other synthetic methods of this type of compound, 4-Iodo-1-trityl-1H-imidazole, and friends who are interested can also refer to it.

Reference:
Patent; REDX PHARMA PLC; ARMER, Richard; BINGHAM, Matilda; PESNOT, Thomas; (84 pag.)WO2016/59412; (2016); A1;,

Extended knowledge of 60-56-0

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 60-56-0.

These common heterocyclic compound, 60-56-0, name is 1-Methyl-1H-imidazole-2(3H)-thione, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity,

Add 1-methyl-2-mercaptoimidazole (0.23 g, 2.04 mmol) to a 150 mL round bottom flask with potassium carbonate as the base(0.32g, 2.35mmol), acetonitrile was stirred at 70 C for 30 minutes, then cooled to room temperature and then added to compound III.(0.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 60-56-0.