Continuously updated synthesis method about 1,1′-Thiocarbonyldiimidazole

The synthetic route of 1,1′-Thiocarbonyldiimidazole has been constantly updated, and we look forward to future research findings.

Application of 6160-65-2, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 6160-65-2, name is 1,1′-Thiocarbonyldiimidazole belongs to imidazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below.

In acetonitrile (10 mL) solution of 2-aminothiazole (1.00 g, 9.99 mmol) 1,1′-thiocarbonyl diimidazole (1.78 g, 9.99 mmol) was added under room temperature and argon gas atmosphere, and stirred at 40 degrees C for 2 hours (it became suspension). The residues were collected after settling reaction mixture at 5 degree C for several hours. filtered, washed and dried in vacuum with cold acetonitrile and then hexane to obtain title compound (a light yellow solid, 1.37 g, 6.49 mmol, 65%).

The synthetic route of 1,1′-Thiocarbonyldiimidazole has been constantly updated, and we look forward to future research findings.