Synthetic Route of 930-62-1, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 930-62-1, name is 2,4-Dimethylimidazole belongs to imidazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below.
General procedure: The ILs as illustrated in Scheme 1, including [Ch][Im], [Ch]-[2-MIm], [Ch][4-MIm], [Ch][2,4-DMIm], [Ch][PhO] and[Ch][2-OP], were synthesized by neutralization of cholinehydroxide ([Ch][OH]) with the corresponding proton donors(i.e., imidazole, 2-methyl imidazole, 4-methyl imidazole,2,4-dimethyl imidazole, phenol, and 2-methyl phenol), respectively.In a typical experiment to synthesize [Ch][Im], anethanol solution of [Ch][OH] was mixed with equimolarimidazole, and was then stirred at room temperature for 24 h.Subsequently, ethanol and water were distilled off at 70 C under reduced pressure. The obtained [Ch][Im] was dried inhigh vacuum for 24 h at 70 C to remove possible trace ofwater. The water content of these ILs was determined by using a Karl Fisher titration and found to be less than0.1 wt%. The as-synthesized ILs were characterized byNMR spectroscopy to verify their chemical structures.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2,4-Dimethylimidazole, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Li, Ruipeng; Zhao, Yanfei; Li, Zhiyong; Wu, Yunyan; Wang, Jianji; Liu, Zhimin; Science China Chemistry; vol. 62; 2; (2019); p. 256 – 261;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem