Electric Literature of 1467-16-9, A common heterocyclic compound, 1467-16-9, name is 1H-Imidazole hydrochloride, molecular formula is C3H5ClN2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Solutions of [H(imidazolium)][Cl] (0.048 g, 45 mmol) in 2 mL CH3CN and K2B12F12 (0.10 mg, 0.22 mmol) in 2 mL CH3CN were mixed at room temperature, affording 0.10 g of salt 3 (93% yield). Single-crystal X-ray diffraction analysis confirmed the composition of this salt.
The synthetic route of 1467-16-9 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Belletire, John L.; Schneider, Stefan; Shackelford, Scott A.; Peryshkov, Dmitry V.; Strauss, Steven H.; Journal of Fluorine Chemistry; vol. 132; 11; (2011); p. 925 – 936;,
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem