Solvent-free synthesis of tris(4-hydroxybutyl acrylate) phosphate in the presence of 1-methylimidazole was written by Ilia, Gheorghe;Macarie, Lavinia;Plesu, Nicoleta;Iliescu, Smaranda;Popa, Adriana. And the article was included in Journal of the Iranian Chemical Society in 2018.HPLC of Formula: 35487-17-3 This article mentions the following:
In this paper, we present the synthesis of tris(4-hydroxybutyl acrylate) phosphate using 1-methylimidazole as acid scavenger for hydrochloric acid byproduct, when an ionic liquid is formed. The synthesis was performed in the absence of any organic solvent. The yield is 83% for ester. The phosphate was characterized by 1H-31P NMR and FTIR. The obtained phosphate is appropriate monomer for UV curing in the presence of photoinitiator. The obtained polymer was characterized by thermal anal. and LOI. The results showed good thermal stability and flame retardancy of UV-cured polymer. In the experiment, the researchers used many compounds, for example, 1-Methyl-1H-imidazol-3-ium chloride (cas: 35487-17-3HPLC of Formula: 35487-17-3).
1-Methyl-1H-imidazol-3-ium chloride (cas: 35487-17-3) belongs to imidazole derivatives. Imidazole derivatives generally have good solubility in protic solvents. Simple imidazole derivatives, such as 1H-imidazole, 2-methyl-1H-imidazole, and 1,2-dimethylimidazole, have very high solubility in water. Imidazole derivatives have antibacterial, antifungal and anticancer functionality. It interacts with DNA and also binds to protein and stops cell division.HPLC of Formula: 35487-17-3
Referemce:
Imidazole – Wikipedia,
Imidazole | C3H4N2 – PubChem